tert-butyl peroxyacetate

N,N-Diallyl-N-carbobutoxymethylamine(DACBMA)was synthesized using diallylamine,butyl chloroacetate and K2CO3 as raw materials.

以二烯丙基胺、氯乙酸丁酯和K2CO3为原料,合成了N,N-二烯丙基-N-羰丁氧甲基胺(DACBMA),将油相与水相分离后用无水硫酸镁干燥,再减压蒸馏,收集157~161℃/1 333 Pa的馏分;然后将收集的馏分用6 mol/L的盐酸中和至油相消失,得到N,N-二烯丙基-N-羰丁氧甲基氯化铵(DACBMAC)溶液;或将其溶于无水乙醚,通入干燥氯化氢,可得到固体DACBMAC。

Synthesis of n-butyl chloroacetate catalyzed by an inorganic solid acid;

无机固体酸催化合成氯乙酸正丁酯

Synthesis of n-butyl chloroacetate catyzed by sodium bisulfateunder microwave irradiation;

微波辐射硫酸氢钠催化合成氯乙酸正丁酯

The synthesis conditions of n-butyl chloroacetate were studied applied solid superacid SO42-/TiO2 as catalyst under microwave irradiation.

在微波辐射下,以SO42-/TiO2固体超强酸为催化剂合成氯乙酸正丁酯。